TLC and Column Chromatography- Post Lab 5
Observations:
1. Fluorene traveled further on the TLC plate then the fluorenone.
2. The
samples on the TLC plate were not visible with eyes.
3. After
70% hexane – 30% acetone was added, the yellow band went down faster.
Data:
Test tube 3 had the fluorenone, test tube 2 had fluorene and
the dot label “M” is a mixture of fluorenone and fluorene. Fluorene travel up
more on the TLC plate than fluorenone.
Post-lab Question:
Why does fluorenone travel more slowly than fluorene? Why
does acetone speed up the rate at which fluorenone travels?
Fluorenone has a carbonyl group which means that it is more
polar than fluorene. Since fluorenone is more polar it travel more slowly than
fluorene. Acetone will speed up the rate at which both fluorene andfluorenone travels up the TLC
plate. It will not change the position.
Comments
Post a Comment